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Thermal Preparation Effects on the X-Ray Diffractograms of Compounds Produced During Flue Gas Desulfurization

  • David L. Wertz (a1), Kathleen H. Burns (a1) (a2), Robert W. Keeton (a1) (a3), Eldon Dilie (a4), S. Angelovich and S. Hassette (a5)...

Abstract

The diffractograms of syn-gypsum and of fine gas desulfurization products indicate that CaSO4.2H2O is converted to other phase(s) when heated to 100°C. Syn-hannebachite (CaSO30.5H2O) is unaffected by similar thermal treatment.

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References

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1. Jones, B. F., Lowell, P. S., and Meserole, F. B., “Experimental and theoretical studies of solid solution formation in lime and limestone SO2 scrubbers”, EPA Report 600/2-76-273a.
2. Wertz, D. L., Energy Fuel, 1990 (4) 442.
3. Smith, D. K., Johnson, G., Scheible, A., Johnson, J. L., and Ullman, G., Powder Diff., 1987 (2) 73.
4. Klug, H. P. and Alexander, L., “X-Ray Diffraction Procedures”, Wiley-fnterscience, NY, 1974, p. 360.
5. Wertz, D. L., Smithhart, C. B., and Wertz, S. L., Adv. X-Ray Anal., 1990 (33) 475.
6. Wertz, D. L. and Bissell, M., Energy Fuel, 1994 (8) 613.

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