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Counter Adaptor and Furnace for Weissenberg Camera*

Published online by Cambridge University Press:  06 March 2019

R. A. Young*
Affiliation:
Georgia Institute of Technology, Atlanta, Georgia
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Abstract

A rugged and versatile counter adaptor for a Weissenberg camera is described. It has performed well in two years of daily use which has included collection of intensity vs. temperature data with conventional cold-stream techniques.

Advantage has recently been taken of the adaptor design to mount, directly on the Weissenberg base, a furnace device which blows hot air along the crystal mounting axis. Crystal temperature may be held constant or easily varied over the range up to about 700°C, with no obstruction of the X-ray beams and no readjustment of the furnace position, while the entire zero layer and close-in upper layers are explored.

Type
Research Article
Copyright
Copyright © International Centre for Diffraction Data 1960

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Footnotes

*

Supported in part by the Air Force Office of Scientific Research, Contract No, AF 49(638)-624.

References

1.See, for example: (a) J. Ladell and K. Lowitzsch, “An Automatic Linear Reciprocal Lame Tracking Single Crystal Diffractometer,” Paper G-7 at the Cornell Meeting of the American Crystallographic Association, July, 1959. (b) K. Drenck, H. Diamant, and R. Pepinsky, “SCADAC; Single CrystarAutomatic Dllfractometer and Analog Computer,” Paper G-8 at the Cornel Meeting of the American Crystallographic Association, July, 1959.Google Scholar
2. Peterson, David T. and Void, C. L., “A Counting Method for Measuring Single Crystal Diffraction Intensities Using a Weissenberg Camera,” Advances in x-ray Analysis, Vol. 1, Plenum Press, New York, 1960, p. 181.Google Scholar
3. Buerger, M. F., X-Ray Crystallography, Wiley, New York, 1942, Chapter 14.Google Scholar